High Resolution NMR in the Solid State: Fundamentals of CP/MAS

Hardcover | November 1, 1995

byE. O. Stejskal, J. D. Memory

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This text was developed from a course for physical chemistry and chemical physics students using cross-polarization (CP) magic angle spinning (MAS) NMR in their laboratory assignments. The book provides students with the details of the CP/MAS experiment as it is used to obtain rare-spin,high-resolution NMR spectra. The design of the CP/MAS experiments and the interpretation of spectra and relaxation measurements require an understanding of the interplay of several fundamental physical interactions not normally encountered in solution NMR. The student can observe the wayinteracting spin systems behave in the solid state, and have a quantum mechanically rigorous understanding of solid-state spin phenomena. The text will have the added benefit of serving as a self-study resource for students seeking to learn the underlying principles of laboratory experiments usingthe technique. The history of NMR is also treated, and the instrumentation of the spectrometer and probe are discussed.

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This text was developed from a course for physical chemistry and chemical physics students using cross-polarization (CP) magic angle spinning (MAS) NMR in their laboratory assignments. The book provides students with the details of the CP/MAS experiment as it is used to obtain rare-spin,high-resolution NMR spectra. The design of the ...

E. O. Stejskal is at North Carolina State University.
Format:HardcoverDimensions:208 pages, 9.57 × 6.3 × 0.79 inPublished:November 1, 1995Publisher:Oxford University Press

The following ISBNs are associated with this title:

ISBN - 10:0195073800

ISBN - 13:9780195073805

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Table of Contents

1. Introduction to NMR Principles2. High Resolution Methods in the Solid State3. Spin-Spin Interactions4. Magic Angle Sample Spinning5. Spectrometer and Probe DesignAppendix A1 Vectors, Matrices, and Complex Numbers. Appendix A2 Geometric Considerations. Appendix A3 Spinning Sidebands. Appendix A4 Average Hamiltonian Theory. Appendix A5 Transmission Lines. Appendix A6 Phase Sensitive Detection. Bibliography.

Editorial Reviews

"A fascinating introduction to the subject ... highly recommend it to those wishing to make the jump from solution NMR. " -- NMR Newsletter