Nmr Case Studies: Data Analysis Of Complicated Molecules

Paperback | March 1, 2017

byJeffrey H Simpson

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NMR Case Studies: Data Analysis of Complicated Molecules provides a detailed discussion of the full logical flow associated with assigning the NMR spectra of complex molecules, also helping readers further develop their NMR spectral assignment skills. The robust case studies present the logic of each assignment, from beginning to end, fully exploring the available range of potential solutions. Readers will gain a better appreciation of various approaches and develop an intuitive sense for when this particular concept should be implemented, thus enhancing their skillsets and providing a host of methodologies potentially amenable to yielding correct assignments. Authored by a scientist with more than 20 years of experience in research and instruction, this book is the ideal reference for anyone in search of application-based content. The book addresses complicated molecules, including corticosteroids, biomolecules, polypeptides, and secondary metabolites. Features the nuclear magnetic resonance NMR spectra of a number of large and interesting molecules, ranging from corticosteroids, to secondary metabolites and large synthetically prepared molecules Uses case studies to pair the spectral signals from the various sites of each molecule to their molecular counterparts in a process called assignment Includes complex NMR problems, aiding readers in the development of NMR spectral assignment skills Features input from a leading scientist with over 20 years of research and instruction experience in the field

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NMR Case Studies: Data Analysis of Complicated Molecules provides a detailed discussion of the full logical flow associated with assigning the NMR spectra of complex molecules, also helping readers further develop their NMR spectral assignment skills. The robust case studies present the logic of each assignment, from beginning to end, ...

From the Jacket

NMR Case Studies: Data Analysis of Complicated Moleculesprovides a detailed discussion of the full logical flow associated with assigning the NMR spectra of complex molecules while helping readers further develop their NMR spectral assignment skills.The robust case studies present the logic of each assignment from beginning to end, and...

Jeffrey H Simpson, PhD, has been the Director of the Instrumentation Facility in the Department of Chemistry at M.I.T. since 2006. Dr. Simpson's career in NMR/instrumentation research and instruction spans 20 years, and he has authored extensively on the subject of NMR. He is also a Founding Member and Vice President of the New England...

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Format:PaperbackDimensions:300 pages, 8.75 × 6.35 × 0.68 inPublished:March 1, 2017Publisher:Elsevier Science & TechLanguage:English

The following ISBNs are associated with this title:

ISBN - 10:0128033428

ISBN - 13:9780128033425

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Table of Contents

I. Basics of 1-D and 2-D NMR Spectroscopy
A. sample
B. Main interaction
C. Perturbations on the Main Interaction
1. Chemical Shift
2. Scalar Coupling (J-Coupling)
3. Dipolar Interaction
4. Dynamic Phenomena and the NMR Time Scale
D. Experiments and their Information Content
1. 1-D 1H
2. 1-D 13C
3. 2-D 1H-1H gCOSY
4. 2-D 1H-13C HSQC
5. 2-D 1H-13C gHMBC
6. 2-D 1H-1H NOESY/EXSY
7. 2-D 1H-1H TOCSY
E. Assignment Strategies and Methodologies
F. Limits of Knowledge
II. Small- and Medium-Sized Molecules (
III. Corticosteroids (
IV. Other Large Molecules (
V. Complex Systems Showing Exchange (<_529_>