Nuclear Magnetic Resonance Spectroscopy in Environmental Chemistry

Hardcover | April 1, 1997

EditorMark A. Nanny, Roger A. Minear, Jerry A. Leenheer

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This book demonstrates the usefulness of NMR spectroscopy for a wide variety of applications in environmental science and technology. It contains a wealth of information relating to instrumentation, sample preparation, and data interpretation. The book is divided into three sectionsdiscussing contaminant interaction, solution and condensed-phase characterization, and nutrients and natural organic matter characterization. In addition to these in-depth chapters, an introductory overview provides the basic principles of solution and solid-state NMR spectroscopy. Each sectionalso contains a discussion of advances in each area directly attributable to NMR spectroscopy. A final chapter suggests future directions for the deployment of this powerful technology in environmental science.

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This book demonstrates the usefulness of NMR spectroscopy for a wide variety of applications in environmental science and technology. It contains a wealth of information relating to instrumentation, sample preparation, and data interpretation. The book is divided into three sectionsdiscussing contaminant interaction, solution and con...

Mark A. Nanny is at University of Illinois, Urbana-Champaign. Roger A. Minear is at University of Illinois, Urbana-Champaign.

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Format:HardcoverDimensions:344 pages, 9.49 × 6.38 × 0.79 inPublished:April 1, 1997Publisher:Oxford University Press

The following ISBNs are associated with this title:

ISBN - 10:0195097513

ISBN - 13:9780195097511

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Table of Contents

IntroductionH. Knicker and M. A. Nanny: Nuclear Magnetic Resonance Spectroscopy: Theory and BackgroundContaminant Interactions1. M. A. Nanny: Sorption Processes in the Environment: Nuclear Magnetic Resonance Spectroscopy as a New Analytical Method2. J. M. Bortiatynski, P. G. Hatcher, and R. D. Minard: The Development of 13C Labeling and 13C NMR Spectroscopy Techniques to Study the Interaction of Pullutants with Humic Substances3. S. J. Anderson: Proton and 19F NMR Spectroscopy of Pesticide Intermolecular Interactions4. B. E. Herbert and P. M. Bertsch: A 19F and 2H NMR Spectroscopic Investigation of the Interaction Between Nonionic Organic Contaminants and Dissolved Humic Material5. D. A. Netzel et al.: Adsorption Isotherms and 13C Solid-state NMR Study of Hazardous Organic Compounds Sorbed on Coal Fly AshSolution and Condensed Phase Characterization6. R. A. Minear and M. A. Nanny: Solution and Condensed Phase Characterization7. F. E. Scully et al.: NMR Studies of the Reaction of Amino Acids with Aqueous Chlorine8. D. V. Vivit, K. A. Thorn, and J. D. Hem: Comparative Results of 27Al NMR Spectrometric and Ferron Colorimetric Analyses of Hydroxyaluminum Hydrolysis Products in Aged, Mildly Acidic, Aqueous Systems9. F. Thomas et al.: 27Al NMR Study of the Hydrolysis and Condensation of Organically Complexed Aluminum10. A. Labouriau, C. T. Johnston, and W. L. Earl: Cation and Water Interaction in the Interlamellae of a Smectite Clay11. J. A. Ripmeester et al.: 2H NMR and Gel Formation of the Ultrafine Solids Fraction Associated with the Athabasca Oil Sands Fine TailsNutrient and Natural Organic Matter Cycling in the Environment12. J. A. Leenheer: Characterization of Natural Organic Matter by Nuclear Magnetic Resonance Spectroscopy13. M. A. Nanny and R. A. Minear: 31P FT-NMR of Concentrated Lake Water Samples14. L. M. Condron, et al.: Use of 31P NMR in the Study of Soils and the Environment15. H. Knicker, R. Frund, and H. -D. Lundemann: Characterization of Nitrogen in Plant Composts and Native Humic Material by Natural-Abundance 15N CPMAS and Solution NMR Spectra16. J. A. Leenheer, T. I. Noyes, and R. L. Wershaw: Acquisition and Interpretation of Liquid State 1H NMR Spectra of Humic and Fulvic Acids17. J. A. Leenheer, G. E. Maciel, and T. I. Noyes: Preparation of Low-Carbon Sediments From the Mississippi River and Certain Tributaries for Solid-state CPMAS 13C NMR Analysis18. M. A. Nanny, R. A. Minear, and J. A. Leenheer: Research Needs for Environmental NMRIndex

Editorial Reviews

"Nuclear magnetic resonance (NMR) spectroscopy has been an important analytical and qualitative tool in chemistry, material science, and organic geochemistry for quite some time, and now is becoming recognized as a valuable tool in environmental science and technology. . . .An introductorychapter is included that reviews the basic principles of solution and solid-state NMR spectroscopy." --Journal of the American Water Resources Association