Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach by Jeffrey H. SimpsonOrganic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach by Jeffrey H. Simpson

Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach

byJeffrey H. SimpsonEditorJeffrey H. Simpson

Paperback | December 30, 2011

Pricing and Purchase Info

$90.99 online 
$105.19 list price save 13%
Earn 455 plum® points

In stock online

Ships free on orders over $25

Not available in stores

about

Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach, Second Edition,is a primary text for a course in two-dimensional (2-D) nuclear magnetic resonance (NMR) techniques, with the goal to learn to identify organic molecular structure. It presents strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra.

The book begins with a discussion of the NMR technique, while subsequent chapters cover instrumental considerations; data collection, processing, and plotting; chemical shifts; symmetry and topicity; through-bond effects; and through-space effects. The book also covers molecular dynamics; strategies for assigning resonances to atoms within a molecule; strategies for elucidating unknown molecular structures; simple and complex assignment problems; and simple and complex unknown problems. Each chapter includes problems that will enable readers to test their understanding of the material discussed. The book contains 30 known and 30 unknown structure determination problems. It also features a supporting website from which instructors can download the structures of the unknowns in selected chapters, digital versions of all figures, and raw data sets for processing.

This book will stand as a single source to which instructors and students can go to obtain a comprehensive compendium of NMR problems of varying difficulty.



  • Presents strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra
  • Contains 30 known and 30 unknown structure determination problems
  • Features a supporting website from which instructors can download the structures of the unknowns in selected chapters, digital versions of all figures, and raw data sets for processing
Title:Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based ApproachFormat:PaperbackDimensions:540 pages, 9.25 × 7.5 × 0.68 inPublished:December 30, 2011Publisher:Academic PressLanguage:English

The following ISBNs are associated with this title:

ISBN - 10:0123849705

ISBN - 13:9780123849700

Look for similar items by category:

Customer Reviews of Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach

Reviews

Table of Contents

PART I: Background and Methods Chapter 1: Introduction Chapter 2: Instrumental Considerations Chapter 3: Data Collection, Processing, and Plotting Chapter 4: 1H and 13C Chemical Shifts Chapter 5: Symmetry and Topicity Chapter 6: Through-Bond Effects: Spin-Spin (J) Coupling Chapter 7: Through-Space Effects: the Nuclear Overhauser Effect (NOE) Chapter 8: Molecular Dynamics Chapter 9: Strategies for Assigning Molecules Chapter 10: Strategies for Elucidating Unknown Molecular Structures PART II: Problems Chapter 11 Simple Assignment Problems Chapter 12: Complex Assignment Problems Chapter 13: Simple Unknown Problems Chapter 14: Complex Unknown Problems Chapter 15: NMR Resonance Assignment Problems Chapter 16: NMR Unknown Problems

Editorial Reviews

"I like [the book] a lot. Books that cover theory in depth AND lots of problems are (surprisingly) rare."--Steven M. Graham, St. John's University"The abundance of problems and highly detailed glossary are especially noteworthy; the quality of the spectrum presentations is excellent [...] Overall organization works well, and the layout and other 'production values' are what one has long come to expect from [Academic Press]."--Barry Shapiro