Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach

Paperback | December 30, 2011

byJeffrey H. SimpsonEditorJeffrey H. Simpson

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Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach, Second Edition, provides an introduction to the use of two-dimensional 2-D nuclear magnetic resonance NMR spectroscopy to determine organic structure. The book begins with a discussion of the NMR technique, while subsequent chapters cover instrumental considerations; data collection, processing, and plotting; chemical shifts; symmetry and topicity; through-bond effects; and through-space effects. The book also covers molecular dynamics; strategies for assigning resonances to atoms within a molecule; strategies for elucidating unknown molecular structures; simple and complex assignment problems; and simple and complex unknown problems. Each chapter includes problems that will enable readers to test their understanding of the material discussed. Presents strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra Contains 30 known and 30 unknown structure determination problems Features a supporting website from which instructors can download the structures of the unknowns in selected chapters, digital versions of all figures, and raw data sets for processing

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From the Publisher

Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach, Second Edition, provides an introduction to the use of two-dimensional 2-D nuclear magnetic resonance NMR spectroscopy to determine organic structure. The book begins with a discussion of the NMR technique, while subsequent chapters cover instrumental...

From the Jacket

Ideal for advanced undergraduate and graduate courses in organic spectroscopy, this book provides the analytical skills and methodologies needed to assign nuclear magnetic resonances to known and unknown molecular structures. Part I covers the essential knowledge along with worked examples synthetic organic chemists should possess to u...

Format:PaperbackDimensions:540 pages, 9.25 × 7.5 × 0.68 inPublished:December 30, 2011Publisher:Academic PressLanguage:English

The following ISBNs are associated with this title:

ISBN - 10:0123849705

ISBN - 13:9780123849700

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Table of Contents

PART I: Background and Methods Chapter 1: Introduction Chapter 2: Instrumental Considerations Chapter 3: Data Collection, Processing, and Plotting Chapter 4: 1H and 13C Chemical Shifts Chapter 5: Symmetry and Topicity Chapter 6: Through-Bond Effects: Spin-Spin (J) Coupling Chapter 7: Through-Space Effects: the Nuclear Overhauser Effect (NOE) Chapter 8: Molecular Dynamics Chapter 9: Strategies for Assigning Molecules Chapter 10: Strategies for Elucidating Unknown Molecular Structures PART II: Problems Chapter 11 Simple Assignment Problems Chapter 12: Complex Assignment Problems Chapter 13: Simple Unknown Problems Chapter 14: Complex Unknown Problems Chapter 15: NMR Resonance Assignment Problems Chapter 16: NMR Unknown Problems

Editorial Reviews

"I like [the book] a lot. Books that cover theory in depth AND lots of problems are (surprisingly) rare."--Steven M. Graham, St. John's University"The abundance of problems and highly detailed glossary are especially noteworthy; the quality of the spectrum presentations is excellent [...] Overall organization works well, and the layout and other 'production values' are what one has long come to expect from [Academic Press]."--Barry Shapiro