The Assignment of the Absolute Configuration by NMR Using Chiral Derivatizing Agents: A Practical…

Hardcover | June 24, 2015

byJose M. Seco, Emilio Quinoa, Ricardo Riguera

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Nuclear magnetic resonance spectroscopy (NMR spectroscopy) is a research technique that uses the magnetic properties of atomic nuclei to determine physical and chemical properties of atoms or the molecules in which they are contained. Proton NMR (1H NMR) is a technique that applies NMRspectroscopy specifically to the hydrogen-1 nuclei within the molecules of a substance, in order to determine the structure of that substance's molecules. The use of 1H NMR for the assignment of absolute configuration of organic compounds is a well-established technique. Recent research describesthe technique's application to mono-, bi- and trifunctional compounds. In addition, several new auxiliary reagents, mono- and biderivatization procedures, on-resin methodologies and more recently, the use of 13C NMR, have been introduced to the field. In The Assignment of the Absolute Configuration by NMR Using Chiral Derivatizing Agents: A Practical Guide, eminent Professor of Organic Chemistry Ricardo Riguera organizes this cutting-edge NMR research. Professor Riguera offers a short and usable guide that introduces the reader to the researchwith a plethora of details and examples. The book briefly explains the theoretical aspects necessary for understanding the methodology, dedicating most of its space to covering the practical aspects of the assignment, with examples and spectra taken from the authors' own experiments. Upper-levelundergraduates, graduate students, and chemical researchers will find this guide useful for their studies and practice.

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Nuclear magnetic resonance spectroscopy (NMR spectroscopy) is a research technique that uses the magnetic properties of atomic nuclei to determine physical and chemical properties of atoms or the molecules in which they are contained. Proton NMR (1H NMR) is a technique that applies NMRspectroscopy specifically to the hydrogen-1 nuclei ...

Ricardo Riguera is Professor of Organic Chemistry at the University of Santiago. He is the author of 200 papers and patents covering bioactive natural products, medicinal chemistry and NMR methods for determination of absolute configuration.

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Format:HardcoverDimensions:264 pages, 9.21 × 6.3 × 0.79 inPublished:June 24, 2015Publisher:Oxford University PressLanguage:English

The following ISBNs are associated with this title:

ISBN - 10:0199996806

ISBN - 13:9780199996803

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Table of Contents

1. The theoretical basis for the assignment by NMR2. Practical aspects for the preparation of the derivatives3. Assignment of the absolute configuration of monofunctionalcompounds by double derivatization4. Assignment of the absolute configuration of monofunctional compounds by single derivatization5. Assignment of the absolute configuration of polyfunctional compounds6. Exercises